Douglas Alpenstock wrote:
Haha, true, freeze distillation of booze has been used for centuries. I had some dodgy homemade wine once and tried it. I seem to recall that the ice formed a pretty solid block. (And the wine was more boozy, but still dodgy.)
I'm careful to call it fractionally freezing and never freeze distilling because;
A) the methanol seems to melt the ice it is in contact with. Yes the cider is mostly a hard block coming out of the freezer, but when you pour off the alcohol it takes some water with it. I suspect you could not use freezing to produce anhydrous methanol so it would not qualify technically (just guessing here).
B) more importantly, if you call something distilling, you invite undue attention from the department of making you sad...
C) almost forgot, FFing does not purify the methanol- the resulting smaller quantity will contain as much of the nasty chemicals that can attack the optic nerve and whatever else as were in the starting quantity.