Orange oil.
I made it with some students one time. We used distillation apparatus and boiled the orange peel with water. Collected the evaporating water and cooled it, condensed it using a Leibig condenser. Then poured the liquid distillate into a burette. The oil floated, and we ran the water out the bottom of the burette and were left with the oil.
We produced less than 1ml in a 2 hour
class.
